{"id":19517,"date":"2018-03-09T09:08:31","date_gmt":"2018-03-09T09:08:31","guid":{"rendered":"https:\/\/www.deberes.net\/tesis\/sin-categoria\/compuestos-ciclometalados-de-pdii-y-ptii-con-ligandos-con-atomos-donadores-de-azufre\/"},"modified":"2018-03-09T09:08:31","modified_gmt":"2018-03-09T09:08:31","slug":"compuestos-ciclometalados-de-pdii-y-ptii-con-ligandos-con-atomos-donadores-de-azufre","status":"publish","type":"post","link":"https:\/\/www.deberes.net\/tesis\/quimica\/compuestos-ciclometalados-de-pdii-y-ptii-con-ligandos-con-atomos-donadores-de-azufre\/","title":{"rendered":"Compuestos ciclometalados de pd(ii) y pt(ii) con ligandos con \u00e1tomos donadores de azufre"},"content":{"rendered":"<h2>Tesis doctoral de <strong> Dar\u00edo Lata Blanco <\/strong><\/h2>\n<p>El presente trabajo se plante\u00f3 como parte de las investigaciones en curso sobre reacciones de ciclometalaci\u00f3n de tiosemicarbazonas como ligandos potencialmente terdentados (c, n, s). Para este estudio se utilizaron los siguientes ligandos, sintetizados mediante condensaci\u00f3n de 4-metilbenzaldeh\u00eddo, 2-metilbenzaldeh\u00eddo, pirrol-2-carboxaldeh\u00eddo y 2-acetilfurano con las siguientes tiosemicarbacidas: t iosemicarbazida, 4-metil-3-tiosemicarbazida, 4-etil-3-tiosemicarbazida.  estos ligandos se hicieron reaccionar con sales de pd(ii) y pt(ii) con objeto de obtener los correspondientes compuestos ciclometalados. Las sales empleadas fueron las siguientes: tetracloropaladato pot\u00e1sico, tetracloropaladato de litio, acetato de paladio, dimetil (1,5-ciclooctadieno) plantino(ii).  los compuestos obtenidos se hicieron reaccionar con difosfinas terciarias en relaci\u00f3n 1:2 y 1:4, trifenilfosfina en relaci\u00f3n 1:4 y un complejo de wolframio, w(co)5dppm, en relaci\u00f3n 1:4. Las difosfinas empleadas fueron las siguientes: 1,2-bis(difenilfosfina)etano  (dppe),  1,3-bis(difenilfosfina)propano (dppp),  1,4-bis(difenilfosfina)butano  (dppb),   bis(difenilfosfina)metano (dppm), 1,1-bis(difenilfosfina)eteno (vdpp).  todos los compuestos obtenidos han sido caracterizados mediante las siguientes t\u00e9cnicas: an\u00e1lisis elemental (c, n, h y s), espectroscopia infrarroja, espectroscopia de resonancia magn\u00e9tica nuclear de 1h, 31p-i1h) y 13c-(1h) y an\u00e1lisis estructural por difracci\u00f3n de rayos x.<\/p>\n<p>&nbsp;<\/p>\n<h3>Datos acad\u00e9micos de la tesis doctoral \u00ab<strong>Compuestos ciclometalados de pd(ii) y pt(ii) con ligandos con \u00e1tomos donadores de azufre<\/strong>\u00ab<\/h3>\n<ul>\n<li><strong>T\u00edtulo de la tesis:<\/strong>\u00a0 Compuestos ciclometalados de pd(ii) y pt(ii) con ligandos con \u00e1tomos donadores de azufre <\/li>\n<li><strong>Autor:<\/strong>\u00a0 Dar\u00edo Lata Blanco <\/li>\n<li><strong>Universidad:<\/strong>\u00a0 Santiago de compostela<\/li>\n<li><strong>Fecha de lectura de la tesis:<\/strong>\u00a0 18\/10\/2002<\/li>\n<\/ul>\n<p>&nbsp;<\/p>\n<h3>Direcci\u00f3n y tribunal<\/h3>\n<ul>\n<li><strong>Director de la tesis<\/strong>\n<ul>\n<li>Jos\u00e9 Manuel Vila Abad<\/li>\n<\/ul>\n<\/li>\n<li><strong>Tribunal<\/strong>\n<ul>\n<li>Presidente del tribunal:  Garc\u00eda v\u00e1zquez Jos\u00e9 arturo <\/li>\n<li>gabriel Garc\u00eda herbosa (vocal)<\/li>\n<li>Jos\u00e9 tom\u00e1s Cuenca agreda (vocal)<\/li>\n<li>Alberto Fern\u00e1ndez l\u00f3pez (vocal)<\/li>\n<\/ul>\n<\/li>\n<\/ul>\n<p>&nbsp;<\/p>\n","protected":false},"excerpt":{"rendered":"<p>Tesis doctoral de Dar\u00edo Lata Blanco El presente trabajo se plante\u00f3 como parte de las investigaciones en curso sobre reacciones [&hellip;]<\/p>\n","protected":false},"author":1,"featured_media":0,"comment_status":"open","ping_status":"open","sticky":false,"template":"","format":"standard","meta":{"site-sidebar-layout":"default","site-content-layout":"","ast-site-content-layout":"","site-content-style":"default","site-sidebar-style":"default","ast-global-header-display":"","ast-banner-title-visibility":"","ast-main-header-display":"","ast-hfb-above-header-display":"","ast-hfb-below-header-display":"","ast-hfb-mobile-header-display":"","site-post-title":"","ast-breadcrumbs-content":"","ast-featured-img":"","footer-sml-layout":"","theme-transparent-header-meta":"","adv-header-id-meta":"","stick-header-meta":"","header-above-stick-meta":"","header-main-stick-meta":"","header-below-stick-meta":"","astra-migrate-meta-layouts":"default","ast-page-background-enabled":"default","ast-page-background-meta":{"desktop":{"background-color":"var(--ast-global-color-4)","background-image":"","background-repeat":"repeat","background-position":"center center","background-size":"auto","background-attachment":"scroll","background-type":"","background-media":"","overlay-type":"","overlay-color":"","overlay-gradient":""},"tablet":{"background-color":"","background-image":"","background-repeat":"repeat","background-position":"center center","background-size":"auto","background-attachment":"scroll","background-type":"","background-media":"","overlay-type":"","overlay-color":"","overlay-gradient":""},"mobile":{"background-color":"","background-image":"","background-repeat":"repeat","background-position":"center center","background-size":"auto","background-attachment":"scroll","background-type":"","background-media":"","overlay-type":"","overlay-color":"","overlay-gradient":""}},"ast-content-background-meta":{"desktop":{"background-color":"var(--ast-global-color-5)","background-image":"","background-repeat":"repeat","background-position":"center center","background-size":"auto","background-attachment":"scroll","background-type":"","background-media":"","overlay-type":"","overlay-color":"","overlay-gradient":""},"tablet":{"background-color":"var(--ast-global-color-5)","background-image":"","background-repeat":"repeat","background-position":"center center","background-size":"auto","background-attachment":"scroll","background-type":"","background-media":"","overlay-type":"","overlay-color":"","overlay-gradient":""},"mobile":{"background-color":"var(--ast-global-color-5)","background-image":"","background-repeat":"repeat","background-position":"center center","background-size":"auto","background-attachment":"scroll","background-type":"","background-media":"","overlay-type":"","overlay-color":"","overlay-gradient":""}},"footnotes":""},"categories":[863,17,20,977],"tags":[59906,59904,39530,59905,35073,18896],"class_list":["post-19517","post","type-post","status-publish","format-standard","hentry","category-compuestos-organometalicos","category-quimica","category-quimica-inorganica","category-santiago-de-compostela","tag-alberto-fernandez-lopez","tag-dario-lata-blanco","tag-gabriel-garcia-herbosa","tag-garcia-vazquez-jose-arturo","tag-jose-manuel-vila-abad","tag-jose-tomas-cuenca-agreda"],"_links":{"self":[{"href":"https:\/\/www.deberes.net\/tesis\/wp-json\/wp\/v2\/posts\/19517","targetHints":{"allow":["GET"]}}],"collection":[{"href":"https:\/\/www.deberes.net\/tesis\/wp-json\/wp\/v2\/posts"}],"about":[{"href":"https:\/\/www.deberes.net\/tesis\/wp-json\/wp\/v2\/types\/post"}],"author":[{"embeddable":true,"href":"https:\/\/www.deberes.net\/tesis\/wp-json\/wp\/v2\/users\/1"}],"replies":[{"embeddable":true,"href":"https:\/\/www.deberes.net\/tesis\/wp-json\/wp\/v2\/comments?post=19517"}],"version-history":[{"count":0,"href":"https:\/\/www.deberes.net\/tesis\/wp-json\/wp\/v2\/posts\/19517\/revisions"}],"wp:attachment":[{"href":"https:\/\/www.deberes.net\/tesis\/wp-json\/wp\/v2\/media?parent=19517"}],"wp:term":[{"taxonomy":"category","embeddable":true,"href":"https:\/\/www.deberes.net\/tesis\/wp-json\/wp\/v2\/categories?post=19517"},{"taxonomy":"post_tag","embeddable":true,"href":"https:\/\/www.deberes.net\/tesis\/wp-json\/wp\/v2\/tags?post=19517"}],"curies":[{"name":"wp","href":"https:\/\/api.w.org\/{rel}","templated":true}]}}