{"id":33777,"date":"1998-01-01T00:00:00","date_gmt":"1998-01-01T00:00:00","guid":{"rendered":"https:\/\/www.deberes.net\/tesis\/sin-categoria\/complejos-metalicos-con-arenofosfinotioles\/"},"modified":"1998-01-01T00:00:00","modified_gmt":"1998-01-01T00:00:00","slug":"complejos-metalicos-con-arenofosfinotioles","status":"publish","type":"post","link":"https:\/\/www.deberes.net\/tesis\/quimica\/complejos-metalicos-con-arenofosfinotioles\/","title":{"rendered":"Complejos metalicos con arenofosfinotioles."},"content":{"rendered":"<h2>Tesis doctoral de <strong>  Perez Lourido Paulo Antonio <\/strong><\/h2>\n<p>Se describe la s\u00edntesis de compuestos de elementos de transici\u00f3n as\u00ed como de los grupos 12, 13 y 14 del sistema peri\u00f3dico, con ligandos arenofosfinotioles, de forma abreviada rp-(sh)x, x=1 \u00f3 2, caracterizados por presentar \u00e1tomos de azufre tiolato y de f\u00f3sforo como \u00e1tomos dadores. Estos ligandos fueron previamente sintetizados por reacci\u00f3n entre bencenotiol y el cloruro de fosfina correspondiente. Para la s\u00edntesis de los complejos met\u00e1licos se han seguido dos m\u00e9todos diferentes. El primero supone un procedimiento electroqu\u00edmico en el que el metal constituye el \u00e1nodo de una celda electroqu\u00edmica que contiene al ligando susceptible de ser reducido en el c\u00e1todo. De esta forma se han obtenido compuestos de fe, co, ni, cu, ag, zn, cd, in, tl y pb. Por otra parte se han obtenido complejos organoest\u00e1nnicos as\u00ed como complejos de renio siguiendo procedimientos est\u00e1ndar.  todos los compuestos obtenidos han sido caracterizados estructuralmente por an\u00e1lisis elemental, espectroscop\u00eda ir, espectrometr\u00eda de masas y en muchos de los casos mediante t\u00e9cnicas difracci\u00f3n de rayos x, lo que permiti\u00f3 deducir las formas de coordinarse del ligando al centro met\u00e1lico as\u00ed como la estereoqu\u00edmica que presenta el compuesto. Tambi\u00e9n han sido llevados a cabo estudios en disoluci\u00f3n mediante la realizaci\u00f3n de sus espectros de resonancia magn\u00e9tico nuclear de 1h, 13c y 31p pudi\u00e9ndose deducir un car\u00e1cter no disociativo por parte de los diferentes compuestos estudiados.<\/p>\n<p>&nbsp;<\/p>\n<h3>Datos acad\u00e9micos de la tesis doctoral \u00ab<strong>Complejos metalicos con arenofosfinotioles.<\/strong>\u00ab<\/h3>\n<ul>\n<li><strong>T\u00edtulo de la tesis:<\/strong>\u00a0 Complejos metalicos con arenofosfinotioles. <\/li>\n<li><strong>Autor:<\/strong>\u00a0  Perez Lourido Paulo Antonio <\/li>\n<li><strong>Universidad:<\/strong>\u00a0 Santiago de compostela<\/li>\n<li><strong>Fecha de lectura de la tesis:<\/strong>\u00a0 01\/01\/1998<\/li>\n<\/ul>\n<p>&nbsp;<\/p>\n<h3>Direcci\u00f3n y tribunal<\/h3>\n<ul>\n<li><strong>Director de la tesis<\/strong>\n<ul>\n<li>Antonio Sousa Alonso<\/li>\n<\/ul>\n<\/li>\n<li><strong>Tribunal<\/strong>\n<ul>\n<li>Presidente del tribunal:  Garc\u00eda V\u00e1zquez Jos\u00e9 Arturo <\/li>\n<li>Luis Antonio Oro Giral (vocal)<\/li>\n<li> Zubieta Eguskiza Jon Kar (vocal)<\/li>\n<li>Pilar Gonzalez Duarte (vocal)<\/li>\n<\/ul>\n<\/li>\n<\/ul>\n<p>&nbsp;<\/p>\n","protected":false},"excerpt":{"rendered":"<p>Tesis doctoral de Perez Lourido Paulo Antonio Se describe la s\u00edntesis de compuestos de elementos de transici\u00f3n as\u00ed como de [&hellip;]<\/p>\n","protected":false},"author":1,"featured_media":0,"comment_status":"open","ping_status":"open","sticky":false,"template":"","format":"standard","meta":{"site-sidebar-layout":"default","site-content-layout":"","ast-site-content-layout":"","site-content-style":"default","site-sidebar-style":"default","ast-global-header-display":"","ast-banner-title-visibility":"","ast-main-header-display":"","ast-hfb-above-header-display":"","ast-hfb-below-header-display":"","ast-hfb-mobile-header-display":"","site-post-title":"","ast-breadcrumbs-content":"","ast-featured-img":"","footer-sml-layout":"","theme-transparent-header-meta":"","adv-header-id-meta":"","stick-header-meta":"","header-above-stick-meta":"","header-main-stick-meta":"","header-below-stick-meta":"","astra-migrate-meta-layouts":"default","ast-page-background-enabled":"default","ast-page-background-meta":{"desktop":{"background-color":"var(--ast-global-color-4)","background-image":"","background-repeat":"repeat","background-position":"center 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