{"id":57701,"date":"2018-03-09T22:45:32","date_gmt":"2018-03-09T22:45:32","guid":{"rendered":"https:\/\/www.deberes.net\/tesis\/sin-categoria\/nuevas-aportaciones-a-la-determinacion-de-aminoglucosidos-mediante-tecnicas-cromatograficos-con-deteccion-luminiscente\/"},"modified":"2018-03-09T22:45:32","modified_gmt":"2018-03-09T22:45:32","slug":"nuevas-aportaciones-a-la-determinacion-de-aminoglucosidos-mediante-tecnicas-cromatograficos-con-deteccion-luminiscente","status":"publish","type":"post","link":"https:\/\/www.deberes.net\/tesis\/analisis-bioquimico\/nuevas-aportaciones-a-la-determinacion-de-aminoglucosidos-mediante-tecnicas-cromatograficos-con-deteccion-luminiscente\/","title":{"rendered":"Nuevas aportaciones a la determinaci\u00f3n de aminogluc\u00f3sidos mediante t\u00e9cnicas cromatogr\u00e1ficos con detecci\u00f3n luminiscente"},"content":{"rendered":"<h2>Tesis doctoral de <strong>  Serrano Rodriguez Juan  Manuel <\/strong><\/h2>\n<p>La presente tesis doctoral aborda diferentes aspectos qu\u00edmico anal\u00edticos relacionados con la determinaci\u00f3n de la familia de antibi\u00f3ticos conocida como amingoluc\u00f3sidos. El estudio anal\u00edtico de estas sustancias no s\u00f3lo se limita al nivel cl\u00ednico o farmac\u00e9utico, su utilidad humana y veterinaria puede ocasionar fen\u00f3menos de contaminaci\u00f3n emergente en zonas de cultivo y regad\u00edo, por lo que su efecto medioambiental es otro aspecto a tener en cuenta. Las investigaciones desarrolladas pueden dividirse en tres secciones, correspondientes cada una, a t\u00e9cnicas y metodolog\u00edas diferentes.     desarrollo de metodolog\u00edas cromatogr\u00e1ficas con detecci\u00f3n quimiluminiscente basadas en el efecto inhibidor de estos antibi\u00f3ticos sobre la reacci\u00f3n de oxidaci\u00f3n del luminol por el per\u00f3xido de hidr\u00f3geno, debido a la capacidad de formaci\u00f3n de quelatos estables con el i\u00f3n cu(ii), catalizador. La metodolog\u00eda desarrollada es r\u00e1pida, sencilla y aporta elevados niveles de sensibilidad expresados como bajos l\u00edmites de detecci\u00f3n del orden de pocos ug\/l. Se ha aplicado con excelentes resultados a la determinaci\u00f3n de estos antibi\u00f3ticos en plasma y orina, as\u00ed como en diferentes tipos de agua.     puesta a punto de m\u00e9todos electrofor\u00e9ticos para la determinaci\u00f3n de antibi\u00f3ticos aminogluc\u00f3sidos y beta-lact\u00e1micos mediante cromatograf\u00eda electrocin\u00e9tica micelar con detecci\u00f3n mediante fluorescencia inducida por l\u00e1ser. Como etapa previa a la separaci\u00f3n ambos tipos de antibi\u00f3ticos se derivatizan haciendo uso del marcador cy5 nhs-\u00e9ster a temperatura ambiente y en tan s\u00f3lo 20 min. Las metodolog\u00edas desarrolladas se aplicaron a la determinaci\u00f3n de mainogluc\u00f3sidos en muestras de leche bovina (l\u00edmites de detecci\u00f3n de pocos ug\/kg y recuperaciones superiores al 89%) y beta-lact\u00e1micos en diferentes muestras de agua, con buenos resultados a nivel de sensibilidad y precisi\u00f3n.     la utilizaci\u00f3n de herramientas quimiom\u00e9tricas en qu\u00edmica anal\u00edtica es un campo de c<\/p>\n<p>&nbsp;<\/p>\n<h3>Datos acad\u00e9micos de la tesis doctoral \u00ab<strong>Nuevas aportaciones a la determinaci\u00f3n de aminogluc\u00f3sidos mediante t\u00e9cnicas cromatogr\u00e1ficos con detecci\u00f3n luminiscente<\/strong>\u00ab<\/h3>\n<ul>\n<li><strong>T\u00edtulo de la tesis:<\/strong>\u00a0 Nuevas aportaciones a la determinaci\u00f3n de aminogluc\u00f3sidos mediante t\u00e9cnicas cromatogr\u00e1ficos con detecci\u00f3n luminiscente <\/li>\n<li><strong>Autor:<\/strong>\u00a0  Serrano Rodriguez Juan  Manuel <\/li>\n<li><strong>Universidad:<\/strong>\u00a0 C\u00f3rdoba<\/li>\n<li><strong>Fecha de lectura de la tesis:<\/strong>\u00a0 27\/03\/2007<\/li>\n<\/ul>\n<p>&nbsp;<\/p>\n<h3>Direcci\u00f3n y tribunal<\/h3>\n<ul>\n<li><strong>Director de la tesis<\/strong>\n<ul>\n<li>Manuel Silva Rodriguez<\/li>\n<\/ul>\n<\/li>\n<li><strong>Tribunal<\/strong>\n<ul>\n<li>Presidente del tribunal: agustina Gomez hens <\/li>\n<li>Santiago Maspoch andres (vocal)<\/li>\n<li>Luis Camacho delgado (vocal)<\/li>\n<li>\u00e1ngel R\u00edos castro (vocal)<\/li>\n<\/ul>\n<\/li>\n<\/ul>\n<p>&nbsp;<\/p>\n","protected":false},"excerpt":{"rendered":"<p>Tesis doctoral de Serrano Rodriguez Juan Manuel La presente tesis doctoral aborda diferentes aspectos qu\u00edmico anal\u00edticos relacionados con la determinaci\u00f3n [&hellip;]<\/p>\n","protected":false},"author":1,"featured_media":0,"comment_status":"open","ping_status":"open","sticky":false,"template":"","format":"standard","meta":{"site-sidebar-layout":"default","site-content-layout":"","ast-site-content-layout":"","site-content-style":"default","site-sidebar-style":"default","ast-global-header-display":"","ast-banner-title-visibility":"","ast-main-header-display":"","ast-hfb-above-header-display":"","ast-hfb-below-header-display":"","ast-hfb-mobile-header-display":"","site-post-title":"","ast-breadcrumbs-content":"","ast-featured-img":"","footer-sml-layout":"","theme-transparent-header-meta":"","adv-header-id-meta":"","stick-header-meta":"","header-above-stick-meta":"","header-main-stick-meta":"","header-below-stick-meta":"","astra-migrate-meta-layouts":"default","ast-page-background-enabled":"default","ast-page-background-meta":{"desktop":{"background-color":"var(--ast-global-color-4)","background-image":"","background-repeat":"repeat","background-position":"center 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